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TEM
induction furnace
characterization of NiTi
mechanical testing
directional soldification
transmission electron microscope
JEOL NEOARM 200F transmission electron microscope
funded by DFG (Inst 275/391-1)
acceleration voltage
80kV and 200kV
electron beam:
cold field emission gun
resolution
TEM 2,3 Å @ 200kV,
STEM 1 Å @ 200kV
Additional equipment:
STEM Aberration Corrector (atomic resolution < 1 Å in STEM HAADF)
EELS and EDS (atomic resolution)
Double tilt holder
Double tilt heating holder (DensSolution) up to 1300ºC
4k CMOS camera (Gatan OneView with in-situ upgrade)
Analyse:
EDX Double SDD (JEOL Centurio)
count rates up to 100 000 cts/s
energy resolution (122eV at Mn Kα)
EEL Spectrometer (Gatan Continuum) with energy resolution < 0.3eV
STEM (< 1 Å in STEM HAADF) mit folgenden Detektoren
Bright field (BF)
Annular Bright Field (ABF)
Annular Dark Field (ADF)
Secondary and Backscattered Electron (SE/BSE) detectors
4D STEM- Diffraction Mapping with STEM X (up to 300 frames/s)
Diffraction (CBD and NBD)
TEM-sample preparation:
Access to the FEI Helios NanoLab 600i focused ion beam system (FIB) of Prof. Carsten Ronning's group (IFK)
Ion beam polishing: Leica RES 101
Electrolyte beam polishing: Struers TenuPol-5
User rules for the transmission electron microscope
Impressum
© by maaja Design & Konzepte